Ammonium Chloride → HCID 19780247, 화합물

HRID 2081589노트

반응식

HRID 2081589 반응식
[Cl:1][C:2]1[CH:18]=[CH:17][CH:16]=[CH:15][C:3]=1[CH2:4][C:5]1[N:10]=[C:9]([C:11](=[NH:14])OC)[CH:8]=[CH:7][CH:6]=1.[Cl-].[NH4+:20]>C(O)C>[ClH:1].[Cl:1][C:2]1[CH:18]=[CH:17][CH:16]=[CH:15][C:3]=1[CH2:4][C:5]1[N:10]=[C:9]([C:11]([NH2:20])=[NH:14])[CH:8]=[CH:7][CH:6]=1

참가 물질

4

반응물 2

HCID 25517Ammonium ChlorideHCID 53896835HCID 53896835, 화합물

생성물 1

HCID 19780247HCID 19780247, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of methyl 6-(o-chlorobenzyl)-2-picoline imidate 5.5 g, 0.021 moles) and ammonium chloride (1.28 g, 0.024 moles) in ethanol (40 ml) was refluxed for 4 hours. The ethanol was removed in vacuo to give 6-(o-chlorobenzyl)-2-picoline amidine hydrochloride which was used in the final stage without further purification.

후처리

  1. temperaturewas refluxed for 4 hours
  2. customThe ethanol was removed in vacuo

출처 및 근거

ORD 기록
ord-5fbed3513ee54e6bbff1079d2aed26cf
출처 데이터셋
uspto-grants-1993_02
특허 번호
US05185339

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