Acetylacetone → 2,4-Pentanedione, 3-[(4-chloro-3-nitrophenyl)methylene]-

HRID 2081713노트

반응식

HRID 2081713 반응식
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11].[CH3:13][C:14](=[O:19])[CH2:15][C:16](=[O:18])[CH3:17]>>[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[C:15]([C:14](=[O:19])[CH3:13])[C:16](=[O:18])[CH3:17])=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11]

참가 물질

3

반응물 2

HCID 31261AcetylacetoneHCID 855054-Chloro-3-nitrobenzaldehyde

생성물 1

HCID 119577922,4-Pentanedione, 3-[(4-chloro-3-nitrophenyl)methylene]-

실험 절차

The procedure described in Example 1 was repeated by using 1.85 g of 4-chloro-3-nitrobenzaldehyde and 1.5 g of 2,4-pentanedione. Yield 1.32 g, mp 110°-111° C.

출처 및 근거

ORD 기록
ord-973b62faea984df0895090d08c650465
출처 데이터셋
uspto-grants-1993_02
특허 번호
US05185370

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