Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethynylcyclohexane → 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethynylcyclohexane | HCID 70263 | — |
| 반응물 | 2-Iodoadenosine | HCID 169662 | — |
| 반응물 | (Prop-2-yn-1-yl)cyclopentane | HCID 521007 | — |
| 생성물 | 2-(3-Cyclopentyl-1-propyn-1-yl)adenosine | HCID 132348 | 70.3% |
반응 단계
The procedure of Example 1 was repeated except that 1.56 g (3.98 mmol) of 2-iodoadenosine was used as the starting compound and that the cyclohexylacetylene was replaced by 3-cyclopentylpropyne, whereby 1.05 g (2.8 mmol) of crystalline 2-(3-cyclopentyl-1-propynyl)adenosine was obtained (yield: 70.3%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05189027 |
| 출처 데이터셋 | uspto-grants-1993_02 |
| ORD ID | ord-c4dab15d462d4976a7538035653ba803 |
| 출처 메모 | uspto-grants-1993_02 |