Potassium Hydroxide → HCID 12330022, 화합물

반응식

[Cl:1][C:2]1[CH:21]=[CH:20][CH:19]=[C:18]([C:22]([O:24]CC)=[O:23])[C:3]=1[CH2:4][O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][C:13]([O:15]CC)=[O:14])=[CH:8][CH:7]=1.[OH-].[K+]>>[C:22]([C:18]1[C:3]([CH2:4][O:5][C:6]2[CH:11]=[CH:10][C:9]([CH2:12][C:13]([OH:15])=[O:14])=[CH:8][CH:7]=2)=[C:2]([Cl:1])[CH:21]=[CH:20][CH:19]=1)([OH:24])=[O:23]

참가 물질

반응물 2

HCID 14797Potassium Hydroxide

HCID 21269134Ethyl 4-(2-chloro-6-ethoxycarbonylbenzyloxy)phenylacetate

생성물 1

HCID 12330022HCID 12330022, 화합물

실험 절차

Reaction of ethyl 4-(2-chloro-6-ethoxycarbonylbenzyloxy)phenylacetate with potassium hydroxide as described in Example 1c provides 4-(6-carboxy-2-chlorobenzyloxy)phenylacetic acid as a colorless solid, mp 171°-173° C.

출처 및 근거

ORD 기록: ord-34eceeb3c7484e92ac89d094e01191b6
출처 데이터셋: uspto-grants-1978_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04082850

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