Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 1-Aminooctan-2-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 2-Hexyloxirane | HCID 18126 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-Aminooctan-2-ol | HCID 345053 | 77.1% |
반응 단계
One-thousand one-hundred grams of ammonia gas was introduced into a mixture of 6 liters of ethanol and 1 liter of water and within 30 minutes there were dropped in at room temperature 320 grams of 1,2-epoxyoctane. The mixture was left at room temperature for 70 minutes under gentle stirring, then the solvent and excess ammonia drawn off and the residue rectified in a vacuum. There were obtained 277.6 grams (77.1% of theory) of 2-hydroxyoctyl amine having a boiling point (0.4 mm Hg) of 80° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04083872 |
| 출처 데이터셋 | uspto-grants-1978_04 |
| ORD ID | ord-a53569f20ab84a23b2282a89ee4cc7a9 |
| 출처 메모 | uspto-grants-1978_04 |