2-Bromo-1-methyl-1H-imidazole → 4-Methoxy-2-(1-methylimidazol-2-yl)benzo(b)furan
반응식
[CH3:1][O:2][C:3]1[C:11]2[CH:10]=[C:9]([Sn](C)(C)C)[O:8][C:7]=2[CH:6]=[CH:5][CH:4]=1.Br[C:17]1[N:18]([CH3:22])[CH:19]=[CH:20][N:21]=1>>[CH3:1][O:2][C:3]1[C:11]2[CH:10]=[C:9]([C:17]3[N:18]([CH3:22])[CH:19]=[CH:20][N:21]=3)[O:8][C:7]=2[CH:6]=[CH:5][CH:4]=1참가 물질
3
실험 절차
By the reactions in the same manner as in Starting Material Synthesis Example 87 using 4-methoxy-2-(trimethylstannyl)benzo(b)furan (5.26 g), 2-bromo-1-methylimidazole (2.72 g) and bistriphenylphosphinepalladium dichloride (593 mg), the title compound (2.06 g) was obtained as a yellow oil.
출처 및 근거
- ORD 기록
- ord-64415c78ca634ee7b95341f8fb00dc38
- 출처 데이터셋
- uspto-grants-2004_04
- 특허 번호
- US06720320B2
반응 노트
불러오는 중…