참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Cyclohexanone | HCID 7967 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Benzaldehyde, 4-[[2-(acetyloxy)ethyl]ethylamino]- | HCID 11458991 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2,6-Bis((4-(ethyl(2-hydroxyethyl)amino)phenyl)methylene)cyclohexan-1-one | HCID 69618590 | 185.2% |
반응 단계
23.5 g of 2-(ethyl(4-formylphenyl)amino)ethyl acetate, 4.91 g of cyclohexanone and 150 ml of ethanol were mixed and to this was added an aqueous solution (25 ml) of 2.2 g of sodium hydroxide while stirring at 50° C. This mixture was further stirred for 5 hours. After cooling to room temperature, a precipitate was filtrated, and washed with a small amount of ethanol and water to obtain 41.5 g of 2,6-bis((4-(ethyl(2-hydroxyethyl)amino)phenyl)methylene)cyclohexan-1-one.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06727037B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_04 |
|---|
| ORD ID | ord-3c148860a4c74c1481c444b95592535e |
|---|
| 출처 메모 | uspto-grants-2004_04 |
|---|
