4'-Fluoroacetophenone → 4-Fluorophenylglyoxal hydrate

반응식

O.[C:2]1([C:8]([CH:10]=[O:11])=[O:9])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[F:12]C1C=CC(C(=O)C)=CC=1>>[OH2:9].[F:12][C:5]1[CH:6]=[CH:7][C:2]([C:8]([CH:10]=[O:11])=[O:9])=[CH:3][CH:4]=1

참가 물질

반응물 2

HCID 98284'-Fluoroacetophenone

HCID 12215922Glyoxal, phenyl-, hydrate

생성물 1

HCID 27374704-Fluorophenylglyoxal hydrate

실험 절차

The title compound was prepared using essentially the same procedure as described by H. A. Riley and A. R. Gray in Organic Synthesis, Collective Volume II, p. 509 for the preparation of phenylglyoxal hydrate, but using 4′-fluoroacetophenone in place of acetophenone.

출처 및 근거

ORD 기록: ord-518d1a45cbd74b60a796d8dc569cf6db
출처 데이터셋: uspto-grants-2004_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06727244B2

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