Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbon Dioxide → HCID 131728205, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbon Dioxide | HCID 280 | — |
| 반응물 | Methanesulfonic Acid | HCID 6395 | — |
| 반응물 | 1-Vinylimidazole | HCID 66171 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 131728205 | HCID 131728205 | 95% |
반응 단계
First, 7 ml of methanesulfonic acid was added to 10 g of N-vinylimidazole, and the resultant mixture was stirred for 3 hours at a temperature kept at 0° C. and then added dropwise to diethyl ether cooled with dry ice. The resultant mixture was rapidly filtered by suction using a Nutsche aspirator provided with a glass filter to recover crystals on the glass filter. The crystals were dried to obtain 19.2 g of N-vinylimidazolium methanesulfonate. The yield was 95%, and the melting point was 5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07746623B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-1125dbe31c5c4f639f50205641e8592e |
| 출처 메모 | uspto-grants-2010_06 |