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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 20888생성일: 2026년 10월 26일

Carbon Dioxide → HCID 131728205, 화합물

https://huagongshe.com/reaction/20888

반응식

참여 물질

역할이름HCID투입량
반응물Carbon DioxideHCID 280—
반응물Methanesulfonic AcidHCID 6395—
반응물1-VinylimidazoleHCID 66171—
용매Diethyl EtherHCID 3283—
생성물HCID 131728205HCID 13172820595%

반응 단계

First, 7 ml of methanesulfonic acid was added to 10 g of N-vinylimidazole, and the resultant mixture was stirred for 3 hours at a temperature kept at 0° C. and then added dropwise to diethyl ether cooled with dry ice. The resultant mixture was rapidly filtered by suction using a Nutsche aspirator provided with a glass filter to recover crystals on the glass filter. The crystals were dried to obtain 19.2 g of N-vinylimidazolium methanesulfonate. The yield was 95%, and the melting point was 5° C.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07746623B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-1125dbe31c5c4f639f50205641e8592e
출처 메모uspto-grants-2010_06