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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2091489생성일: 2026년 10월 23일

Ethanol → 1-Tetradecyl-3-ethylglycerol

https://huagongshe.com/ko/reaction/2091489

반응식

참여 물질

역할이름HCID투입량
반응물EthanolHCID 702—
반응물Oxirane, 2-((tetradecyloxy)methyl)-HCID 38190—
반응물Sodium ethoxideHCID 2723922—
생성물1-Tetradecyl-3-ethylglycerolHCID 86652916319.6%

반응 조건

온도80 °C

반응 단계

Under nitrogen stream, 30 g of sodium ethoxide was added to 851.8 g (18.5 mol) of ethanol, and the mixture was heated to 80° C. Then, 500 g (1.85 mol) of tetradecyl glycidyl ether were added dropwise thereto. The mixture was stirred for 18 hours at the same temperature. Thereafter, ethanol was distilled off, and 10.8 g of 85% phosphoric acid was added thereto, followed by washing the resultant mixture with water three times. After water washing, distillation was performed under reduced pressure, to thereby obtain 446 g of 1-tetradecyl-3-ethylglycerol (yield 76.2%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08440645B2
출처 데이터셋uspto-grants-2013_05
ORD IDord-7de36ed9740c418595431acf70cab376
출처 메모uspto-grants-2013_05