1-(3-Methylphenyl)cyclopropane-1-carbonitrile → m-Methylphenylacetonitrile

HRID 2094672노트

반응식

HRID 2094672 반응식
[C:1]1([CH3:12])[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2([C:10]#[N:11])CC2)[CH:2]=1>CC(=O)OCC>[C:1]1([CH3:12])[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][C:10]#[N:11])[CH:2]=1

참가 물질

3

반응물 1

HCID 200261921-(3-Methylphenyl)cyclopropane-1-carbonitrile

생성물 1

HCID 76279m-Methylphenylacetonitrile

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

After silica gel chromatography of the residue (HEP/EA gradient), an approximately 1:1 mixture of 1-m-tolyl-cyclopropanecarbonitrile and the starting compound m-tolylacetonitrile was obtained.

출처 및 근거

ORD 기록
ord-42940c5a2b9c4cedb7398bc24aa1df5b
출처 데이터셋
uspto-grants-2013_05
특허 번호
US08445530B2

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