Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-((tert-Butyldimethylsilyl)oxy)-4-methoxybenzaldehyde → Methyl 1-(3-(tert-butyldimethylsilyloxy)-4-methoxybenzylamino)cyclopropanecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-((tert-Butyldimethylsilyl)oxy)-4-methoxybenzaldehyde | HCID 359558 | — |
| 반응물 | Methyl 1-aminocyclopropane-1-carboxylate hydrochloride | HCID 12760695 | — |
| 생성물 | Methyl 1-(3-(tert-butyldimethylsilyloxy)-4-methoxybenzylamino)cyclopropanecarboxylate | HCID 59524368 | 79% |
반응 단계
Prepared as in Example 12-1b from 3-(tert-butyldimethylsilyloxy)-4-methoxybenzaldehyde (Example 12-2c) and methyl 1-aminocyclopropanecarboxylate hydrochloride. Yield 79%. MS 366 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08445692B2 |
| 출처 데이터셋 | uspto-grants-2013_05 |
| ORD ID | ord-9947a58501ab483690c928abe5b592fe |
| 출처 메모 | uspto-grants-2013_05 |