1,4-Dioxaspiro[4.5]decan-8-one → HCID 59361629, 화합물

HRID 2096159노트

반응식

HRID 2096159 반응식
Br[C:2]1[CH:3]=[C:4]([CH3:10])[C:5]([O:8][CH3:9])=[N:6][CH:7]=1.[O:11]1[C:15]2([CH2:20][CH2:19][C:18](=[O:21])[CH2:17][CH2:16]2)[O:14][CH2:13][CH2:12]1>CCOCC>[CH3:9][O:8][C:5]1[N:6]=[CH:7][C:2]([C:18]2([OH:21])[CH2:19][CH2:20][C:15]3([O:14][CH2:13][CH2:12][O:11]3)[CH2:16][CH2:17]2)=[CH:3][C:4]=1[CH3:10]

참가 물질

4

반응물 2

HCID 5674151,4-Dioxaspiro[4.5]decan-8-oneHCID 225911765-Bromo-2-methoxy-3-methylpyridine

생성물 1

HCID 59361629HCID 59361629, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

The title compound was prepared as a white solid from 5-bromo-2-methoxy-3-methyl-pyridine (Alfa Aesar) and 1,4-dioxa-spiro[4.5]decan-8-one in ether using the procedure described in Step A of Example 1.

출처 및 근거

ORD 기록
ord-2fb63e749b114bf5bb3a650496e48c00
출처 데이터셋
uspto-grants-2013_05
특허 번호
US08450304B2

반응 노트

불러오는 중…