Thionyl Chloride → HCID 58424408, 화합물

반응식

[Br:1][C:2]1[CH:14]=[CH:13][C:5]([O:6][CH2:7][CH2:8][CH2:9][C:10](O)=[O:11])=[CH:4][CH:3]=1.O=S(Cl)[Cl:17]>>[Br:1][C:2]1[CH:14]=[CH:13][C:5]([O:6][CH2:7][CH2:8][CH2:9][C:10]([Cl:17])=[O:11])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 23844544-(4-Bromophenoxy)butanoic acid

생성물 1

HCID 58424408HCID 58424408, 화합물수율 67%

실험 절차

4-(4-Bromophenoxy)butanoic acid (39 g, 25.6 mmol) was dissolved in SOCl2(100 ml) mixture was heated to refluxed overnight. the mixture was concentrated in vacuo to give 4-(4-bromophenoxy)butanoyl chloride (27.6 g, 67%).

후처리

temperaturewas heated
temperatureto refluxed overnight
concentrationthe mixture was concentrated in vacuo

출처 및 근거

ORD 기록: ord-96dfd8d2418a45dcbca793d91e1166ea
출처 데이터셋: uspto-grants-2013_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08450308B2

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