2-Methoxyethylamine → N-(2-methoxyethyl)methanesulfonamide
반응식
[CH3:1][O:2][CH2:3][CH2:4][NH2:5].C(N(CC)CC)C.[CH3:13][S:14](Cl)(=[O:16])=[O:15]>ClCCl>[CH3:1][O:2][CH2:3][CH2:4][NH:5][S:14]([CH3:13])(=[O:16])=[O:15]참가 물질
5
실험 절차
To a stirring solution of 2-methoxyethylamine (0.58 ml) in dichloromethane (10 ml) was added triethylamine (1.0 ml) and methanesulphonyl chloride (0.51 ml). The mixture was stirred at room temperature overnight. The solvents were removed in vacuo to give a crude product which was purified by flash chromatography to give N-(2-Methoxy-ethyl)-methanesulfonamide (0.74 g).
후처리
- customThe solvents were removed in vacuo
- customto give a crude product which
- customwas purified by flash chromatography
출처 및 근거
- ORD 기록
- ord-5c533c63910049a7973a3ff144baf9cf
- 출처 데이터셋
- uspto-grants-2013_05
- 특허 번호
- US08450315B2
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