HCID 178468865, 화합물 → HCID 14722178, 화합물

HRID 2099459노트

반응식

HRID 2099459 반응식
[N+]([O-])(O)=O.[CH2:5]([O:7][C:8](=[O:19])[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][CH:16]=[N:17]N)[CH:10]=1)[CH3:6].[N+:20]([O-])(O)=O.C(OC(=O)[C:28]1[CH:33]=[CH:32][C:31]([CH3:34])=[C:30]([NH:35][CH:36]=NN)[CH:29]=1)C>>[CH2:5]([O:7][C:8](=[O:19])[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([NH:15][C:16]2[N:20]=[C:32]([C:33]3[CH:36]=[N:35][CH:30]=[CH:29][CH:28]=3)[CH:31]=[CH:34][N:17]=2)[CH:10]=1)[CH3:6]

참가 물질

3

반응물 2

HCID 178468865HCID 178468865, 화합물HCID 178468911HCID 178468911, 화합물

생성물 1

HCID 14722178HCID 14722178, 화합물

실험 절차

Utilising the procedure described in example 1b but employing 3-[(aminoiminomethyl)amino]-benzoic acid ethyl ester mononitrate in lieu of 3-[(aminoiminomethyl)amino]-4-methyl-benzoic acid ethyl ester mononitrate, afforded the title compound as a crystalline solid, m.p. 197-199° C.

출처 및 근거

ORD 기록
ord-37b246561abf4fedbeaa1e6412b156d3
출처 데이터셋
uspto-grants-2009_08
특허 번호
US07569566B2

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