Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl isocyanate → N-(t-Butyl)-4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole-2-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl isocyanate | HCID 62412 | — |
| 반응물 | 4-(4-Chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole | HCID 22066083 | — |
| 생성물 | N-(t-Butyl)-4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole-2-carboxamide | HCID 10274740 | — |
반응 단계
Using essentially the same procedure as Example 33, but using t-butyl isocyanate (0.040 mL, 0.30 mmol), 4-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-1-methylimidazole (50 mg, 0.15 mmol) from Example 32, Step C was converted to the title compound after purification by Prep TLC (25% ethyl acetate in hexanes).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07572785B2 |
| 출처 데이터셋 | uspto-grants-2009_08 |
| ORD ID | ord-3eeb4acbdbc947baaa2065d87f643db5 |
| 출처 메모 | uspto-grants-2009_08 |