Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloro-4-fluoroanisole → 4-Chloro-2-fluoro-5-methoxybenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloro-4-fluoroanisole | HCID 2773580 | — |
| 반응물 | 4-Chloro-5-ethyl-2-fluorobenzaldehyde | HCID 57803801 | — |
| 생성물 | 4-Chloro-2-fluoro-5-methoxybenzaldehyde | HCID 14928268 | — |
반응 단계
Following the procedure for Intermediate 390.2, 2-chloro-4-fluoro-1-methoxybenzene (1.0 g, 6.3 mmol) afforded 840 mg of Intermediate 392.1 as a white solid. 1H NMR (400 MHz, CDCl3) δ ppm 3.91 (s, 3H) 6.90-7.00 (m, 1H) 7.41 (dd, J=9.35, 6.32 Hz, 1H) 10.27 (s, 1H)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07576098B2 |
| 출처 데이터셋 | uspto-grants-2009_08 |
| ORD ID | ord-cbf9c140bb5848978b2d937d778b9ddc |
| 출처 메모 | uspto-grants-2009_08 |