Potassium Hydroxide → HCID 54375287, 화합물

HRID 2106593노트

반응식

HRID 2106593 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[C:12]([CH3:13])=[N:11][C:10]([O:14][CH:15]([C:17]([O:19]CC)=[O:18])[CH3:16])=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[OH-].[K+]>C(O)C>[C:17]([CH:15]([O:14][C:10]1[N:11]=[C:12]([CH3:13])[N:8]([C:4]2[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[CH:3]=2)[N:9]=1)[CH3:16])([OH:19])=[O:18]

참가 물질

4

반응물 2

HCID 14797Potassium HydroxideHCID 163821Propanoic acid, 2-((1-(3-chlorophenyl)-5-methyl-1H-1,2,4-triazol-3-yl)oxy)-, ethyl ester

생성물 1

HCID 54375287HCID 54375287, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A 3.8 g portion of the compound of Example 17 was refluxed for 4 hours with 1.4 g of potassium hydroxide in 100 ml of ethanol, and the product was collected as shown in Example 22 and recrystallized from ethanol to obtain 2.8 g of the desired product, m.p. 101°-103°.

후처리

  1. customthe product was collected
  2. customrecrystallized from ethanol

출처 및 근거

ORD 기록
ord-b9cd3c313b59421b98ba547d9f94536a
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04931083

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