Sulfuric Acid → HCID 19828702, 화합물

HRID 2107076노트

반응식

HRID 2107076 반응식
[CH:1]([C:3]1([C:12](Cl)=[O:13])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].[CH2:15](OC(=O)CC(O)=O)C.C(O[Mg])C.S(=O)(=O)(O)O>C(OCCCC)CCC>[CH:1]([C:3]1([C:12](=[O:13])[CH3:15])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

참가 물질

5

반응물 3

HCID 1118Sulfuric AcidHCID 53915754HCID 53915754, 화합물HCID 178472270HCID 178472270, 화합물

생성물 1

HCID 19828702HCID 19828702, 화합물

시약·촉매·용매 1

HCID 8909Butyl ether용매

실험 절차

1-(2,3-Dihydro-2-vinyl-1H-inden-2-yl)-ethanone was prepared by treating 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid chloride with ethoxy magnesium malonic acid ethyl ester in dibutylether and after that with sulfuric acid according to the method of Reynolds, G. A. and Hauser, C. B., Org. Synth. 30 (1957) 70.

출처 및 근거

ORD 기록
ord-27d9d52e89424236876298bbbab18709
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933359

반응 노트

불러오는 중…