Ammonia → 5(2-Morpholinothiazol-4-ylmethylene)rhodanine-3-acetic acid
반응식
[O:1]1[CH2:6][CH2:5][N:4]([C:7]2[S:8][CH:9]=[C:10]([CH:12]=O)[N:11]=2)[CH2:3][CH2:2]1.[S:14]1[CH2:20][C:18](=[O:19])[N:17]([CH2:21][C:22]([OH:24])=[O:23])[C:15]1=[S:16].[Cl-].[NH4+].N>C(O)C>[O:1]1[CH2:2][CH2:3][N:4]([C:7]2[S:8][CH:9]=[C:10]([CH:12]=[C:20]3[S:14][C:15](=[S:16])[N:17]([CH2:21][C:22]([OH:24])=[O:23])[C:18]3=[O:19])[N:11]=2)[CH2:5][CH2:6]1참가 물질
6
실험 절차
The reaction described in Example 1 was repeated, but using 1.65 g of 2-morpholinothiazole-4-carbaldehyde, 1.3 g of rhodanine-3-acetic acid, 1g of ammonium chloride, 1 ml of 28% v/v aqueous ammonia and 35 ml of ethanol, giving the title compound as yellow needles.
출처 및 근거
- ORD 기록
- ord-783f4e5138f84a92869f1110e00b3d72
- 출처 데이터셋
- uspto-grants-1990_06
- 특허 번호
- US04933355
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