Ethyl bromopyruvate → HCID 15053539, 화합물

HRID 2107273

반응식

HRID 2107273 반응식
[F:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([NH2:11])=[S:10])=[CH:4][CH:3]=1.Br[CH2:13][C:14](=O)[C:15]([O:17][CH2:18][CH3:19])=[O:16]>C(O)C>[F:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]2[S:10][CH:13]=[C:14]([C:15]([O:17][CH2:18][CH3:19])=[O:16])[N:11]=2)=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 66144Ethyl bromopyruvateHCID 6930614-Fluorophenylthiourea

생성물 1

HCID 15053539HCID 15053539, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The reaction described in Preparation 42 was repeated, but using 12 g of p-fluorophenylthiourea, 14.8 g of ethyl bromopyruvate, and 120 ml of ethanol, giving the title compound as pale yellow prisms.

후처리

  1. customThe reaction described in Preparation 42

출처 및 근거

ORD 기록
ord-76548fe2596748cfb6c7f44ba938a191
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933355

연결된 노트

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