Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate → 2-Allylaminothiazol-4-ylmethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate | HCID 7171906 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-Allylaminothiazol-4-ylmethanol | HCID 15053559 | — |
반응 단계
The reaction described in Preparation 15 was repeated, but using 10 g of ethyl 2-allylaminothiazole-4-carboxylate, 2.7 g of lithium aluminum hydride and 150 ml of tetrahydrofuran. giving the title compound as pale brown needles.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04933355 |
| 출처 데이터셋 | uspto-grants-1990_06 |
| ORD ID | ord-96b70246f9234f0a9c9bdb303be4c2c6 |
| 출처 메모 | uspto-grants-1990_06 |