Ethyl bromopyruvate → Ethyl 2-(cyclohexylamino)-1,3-thiazole-4-carboxylate

HRID 2107284

반응식

HRID 2107284 반응식
[CH:1]1([NH:7][C:8]([NH2:10])=[S:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Br[CH2:12][C:13](=O)[C:14]([O:16][CH2:17][CH3:18])=[O:15]>C(O)C>[CH:1]1([NH:7][C:8]2[S:9][CH:12]=[C:13]([C:14]([O:16][CH2:17][CH3:18])=[O:15])[N:10]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 66144Ethyl bromopyruvateHCID 1471603Cyclohexylthiourea

생성물 1

HCID 15053542Ethyl 2-(cyclohexylamino)-1,3-thiazole-4-carboxylate

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The reaction described in Preparation 42 was repeated, but using 17 g of cyclohexylthiourea, 22 g of ethyl bromopyruvate and 200 ml of ethanol, giving the title compound as a yellow oil.

후처리

  1. customThe reaction described in Preparation 42

출처 및 근거

ORD 기록
ord-6eb112148f5f445fa45f6d001bb24714
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933355

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