HCID 15053543, 화합물 → HCID 15053561, 화합물
반응식
[C:1]1([N:7]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:8]2[S:9][CH:10]=[C:11]([C:13](OCC)=[O:14])[N:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[C:18]1([N:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[C:8]2[S:9][CH:10]=[C:11]([CH2:13][OH:14])[N:12]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1참가 물질
4
실험 절차
The reaction described in Preparation 15 was repeated, but using 27 g of ethyl 2-diphenylaminothiazole-4-carboxylate, 4.7 g of lithium aluminum hydride and 400 ml of tetrahydrofuran, giving the title compound as pale yellow prisms.
후처리
- customThe reaction described in Preparation 15
출처 및 근거
- ORD 기록
- ord-ff9b342d691c47c2a3af3c66986997d2
- 출처 데이터셋
- uspto-grants-1990_06
- 특허 번호
- US04933355
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