Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Bromophenol → HCID 23062453, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Bromophenol | HCID 7808 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3-(Chloromethyl)-1,2,4,5-tetramethylbenzene | HCID 81939 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | HCID 23062453 | HCID 23062453 | 79% |
반응 단계
In acetone (50 ml), a mixture of 4-bromophenol (7.8 g), 2,3,5,6-tetramethylbenzyl chloride (6.3 g) and potassium carbonate (6.5 g) was heated at reflux for 16 hours. The reaction solution was filtered, and the filtrate was concentrated under reduced pressure. The residue was dissolved in ethyl acetate, and successively washed with 3% aqueous sodium hydroxide solution, water and saturated brine. The solvent was evaporated under reduced pressure, thereby giving 8.7 g of the desired compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07514452B2 |
| 출처 데이터셋 | uspto-grants-2009_04 |
| ORD ID | ord-52c09326b92d4d6db679987c70e3e86c |
| 출처 메모 | uspto-grants-2009_04 |