참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-Iodophthalic acid | HCID 238231 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 3-Iodophthalic anhydride | HCID 282071 | 96% |
반응 단계
3-Iodophthalic acid (4.00 g, 13.7 mmol) was dissolved in anhydrous acetic acid, and the solution was stirred at 145° C. for 1 hour. The solvent of the reaction mixture was evaporated under reduced pressure and the residue was purified by slurry using diisopropylether to obtain 3-iodophthalic acid anhydride (3.6 g, yield 96%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07745641B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-2fc0ada1147d4bd8ade7960d2b1c0711 |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
