2-Bromo-4-nitrophenol → 4-Amino-2-bromophenol

HRID 2111854노트

반응식

HRID 2111854 반응식
[Br:1][C:2]1[CH:7]=[C:6]([N+:8]([O-])=O)[CH:5]=[CH:4][C:3]=1[OH:11].[Cl-].[NH4+]>[Fe].CO>[NH2:8][C:6]1[CH:5]=[CH:4][C:3]([OH:11])=[C:2]([Br:1])[CH:7]=1

참가 물질

5

반응물 2

HCID 221092-Bromo-4-nitrophenol2회HCID 25517Ammonium Chloride

생성물 1

HCID 144402654-Amino-2-bromophenol

시약·촉매·용매 2

HCID 23925Iron촉매HCID 887Methanol용매

실험 절차

The target compound was obtained by reducing 2-bromo-4-nitrophenol with iron in a mixed solution of methanol and ammonium chloride aqueous solution. 2-bromo-4-nitrophenol was manufactured by the method described in the literature (J. Org. Chem., Vol. 62, 1997, p. 4504).

후처리

  1. customThe target compound was obtained

출처 및 근거

ORD 기록
ord-c09a539bdb21497a82488acdaa5c9541
출처 데이터셋
uspto-grants-2009_04
특허 번호
US07521455B2

반응 노트

불러오는 중…