Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Methoxide → 2-(3H-imidazo[4,5-b]pyridin-3-ylmethoxy)-ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 반응물 | acetic acid 2-(3H-imidazo[4,5-b]pyridin-3-ylmethoxy)-ethyl ester | HCID 68879998 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-(3H-imidazo[4,5-b]pyridin-3-ylmethoxy)-ethanol | HCID 14464047 | 99% |
반응 단계
0.79 g (3.36 mmol) acetic acid 2-(3H-imidazo[4,5-b]pyridin-3-ylmethoxy)-ethyl ester were dissolved in 10 ml methanol and 10 mg (1.85 mmol) sodium methoxide were added. The mixture was stirred at room temperature for 3 hours. The orange mixture was concentrated in vacuo to afford 0.64 g (99%) of crude product. MS (EI): 193.2, 163.2, 148.2, 133.2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07524823B2 |
| 출처 데이터셋 | uspto-grants-2009_04 |
| ORD ID | ord-6a882374f2714fc8a71d2ed4c286d4ab |
| 출처 메모 | uspto-grants-2009_04 |