Pyridine-3-sulfonyl chloride → 4-(1-Piperazinyl)-1-(3-pyridinylsulfonyl)-1H-indole Hydrochloride

참여 물질

역할	이름	HCID	투입량
반응물	Pyridine-3-sulfonyl chloride	HCID 3164136	—
반응물	tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate	HCID 22015386	—
생성물	4-(1-Piperazinyl)-1-(3-pyridinylsulfonyl)-1H-indole Hydrochloride	HCID 22015331	—

반응 단계

The title compound was prepared from 4-(4-boc-piperazinyl)-indole and 3-pyridinylsulfonyl chloride according to Method 3: 1H NMR (270 MHz, DMSO-d6) δ 9.37 (br, 1H), 9.18 (d, J=3 Hz, 1H), 8.86 (d, J=5 Hz, 1H), 8.39 (d, J=8 Hz, 1H), 7.85 (d, J=3 Hz, 1H), 7.70-7.60 (m, 2H), 7.27 (t, J=8 Hz, 4H), 7.00 (d, J=3 Hz, 1H), 6.82 (d, J=8 Hz, 1H), 3.24 (m, 8H); MS (ESI+) for m/z 343 (M+H)+.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US07524839B2
출처 데이터셋	uspto-grants-2009_04
ORD ID	ord-a7676c7af9104a90af2e59f7707df19e
출처 메모	uspto-grants-2009_04