2-Chlorobenzaldehyde → (2-Amino-4-methoxy-5-(1-methylethoxy)phenyl)-(2-chlorophenyl)-methanone

HRID 2112483노트

반응식

[Cl:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=[O:5].[CH:10]([O:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][C:15]=1[O:21][CH3:22])([CH3:12])[CH3:11]>>[NH2:18][C:17]1[CH:16]=[C:15]([O:21][CH3:22])[C:14]([O:13][CH:10]([CH3:12])[CH3:11])=[CH:20][C:19]=1[C:4]([C:3]1[CH:6]=[CH:7][CH:8]=[CH:9][C:2]=1[Cl:1])=[O:5]

참가 물질

반응물 2

HCID 69962-Chlorobenzaldehyde

HCID 64841973-Methoxy-4-(1-methylethoxy)benzenamine

생성물 1

HCID 57642339(2-Amino-4-methoxy-5-(1-methylethoxy)phenyl)-(2-chlorophenyl)-methanone

실험 절차

(2-amino-4-methoxy-5-(1-methylethoxy)phenyl)-(2-chlorophenyl)-methanone (Xjj) was prepared by reacting 2-chlorobenzaldehyde with 0.0267 moles of 4-isopropoxy-3-methoxy aniline in a manner analogous to Example 1. MH+/Z=320.

출처 및 근거

ORD 기록: ord-3f8c769c288345bb991807155f517d9f
출처 데이터셋: uspto-grants-2009_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07524840B2

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