Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diisobutylaluminumhydride → HCID 178486415, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diisobutylaluminumhydride | HCID 21225700 | — |
| 반응물 | 1-Allyl-5-chloro-3-methyl-1H-pyrazol-4-amine | HCID 57642344 | — |
| 반응물 | (2-Amino-4-methoxy-5-methylphenyl)-(2-chlorophenyl)-methanone | HCID 57642372 | — |
| 반응물 | HCID 178456641 | HCID 178456641 | — |
| 생성물 | HCID 178486415 | HCID 178486415 | — |
반응 단계
5-(2-chlorophenyl)-1,2-dihydro-8-methoxy-3,7-dimethyl-pyrazolo[3,4-b][1,4]benzodiazepine (IVz) was prepared by reacting 0.0012 moles of (2-amino-4-methoxy-5-methylphenyl)-(2-chlorophenyl)-methanone (Xz) with 4-amino-5-chloro-3-methyl-1-(2-propenyl)-1H-pyrazole (XIII), and subsequent dealkylation of the intermediate, 5-(2-chlorophenyl)-1,2-dihydro-8-methoxy-3,7-dimethyl-1-(2-propenyl)-pyrazolo[3,4-b][1,4]benzodiazepine (XIVz) with diisobutylaluminum hydride in a manner analogous to Example 72. MH+/Z=353.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07524840B2 |
| 출처 데이터셋 | uspto-grants-2009_04 |
| ORD ID | ord-7cf710a3d4ed4909b2b45eff27418d49 |
| 출처 메모 | uspto-grants-2009_04 |