참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 반응물 | Sodium Perchlorate | HCID 522606 | — |
| 반응물 | 2-Acetyl-9,10-dimethylanthracene | HCID 12438772 | — |
| 생성물 | 9,10-Dimethylanthracene-2-carboxylic acid | HCID 23109523 | — |
반응 단계
9,10-Dimethyl-2-acetylanthracene (1.2 g) was dissolved in dioxane (24 mL). An aqueous solution of sodium perchlorate (10 mL; effective chlorine concentration: 10 wt %) was then added, followed by reaction under stirring at 85° C. for 8 hours. The reaction mixture was chilled, and then rendered acidic with dilute hydrochloric acid. The resulting precipitate was collected by filtration, washed with a small amount of water, and then dried in vacuo to afford the target compound (1.16 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07524985B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_04 |
|---|
| ORD ID | ord-7c4dfc0e2b814a16996f11fa733920dd |
|---|
| 출처 메모 | uspto-grants-2009_04 |
|---|
