P-Anisidine → 2-(4-Benzyl-piperidin-1-yl)-N-(4-methoxy-phenyl)-2-oxo-acetamide

HRID 2115044

반응식

HRID 2115044 반응식
[CH2:1]([CH:8]1[CH2:13][CH2:12][N:11]([C:14](=[O:18])[C:15]([OH:17])=O)[CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:19][O:20][C:21]1[CH:27]=[CH:26][C:24]([NH2:25])=[CH:23][CH:22]=1>C(OCC)C>[CH2:1]([CH:8]1[CH2:9][CH2:10][N:11]([C:14](=[O:18])[C:15]([NH:25][C:24]2[CH:26]=[CH:27][C:21]([O:20][CH3:19])=[CH:22][CH:23]=2)=[O:17])[CH2:12][CH2:13]1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 7732P-AnisidineHCID 16110264(4-Benzylpiperidin-1-yl)oxoacetic acid

생성물 1

HCID 448920382-(4-Benzyl-piperidin-1-yl)-N-(4-methoxy-phenyl)-2-oxo-acetamide

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

The title compound is prepared from (4-benzyl-piperidin-1-yl)-oxo-acetic acid (Example 5b) and 4-methoxyaniline (Aldrich) according to the method described in Example 1c. Melting Point: 144-146° C. (diethylether)

출처 및 근거

ORD 기록
ord-641a35960eb34fd084672cf00899ad69
출처 데이터셋
uspto-grants-2008_10
특허 번호
US07435744B2

연결된 노트

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