Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-6-chlorobenzaldehyde → (+/-)-(2-Amino-6-chlorophenyl)-cyclopentyl-methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-6-chlorobenzaldehyde | HCID 22399512 | — |
| 반응물 | HCID 178419650 | HCID 178419650 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | (+/-)-(2-Amino-6-chlorophenyl)-cyclopentyl-methanol | HCID 69315836 | 36% |
반응 단계
This compound was prepared using General Method 1 (EXAMPLE 1) from 2-amino-6-chlorobenzaldehyde (0.30 g, 1.9 mmol) and cyclopentylmagnesium bromide (2 M in ether, 1.9 mL)) to afford 0.16 g (36%) of (±)-(2-amino-6-chlorophenyl)-cyclopentyl-methanol after flash chromatography (4:1 hexanes:ethyl acetate).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07442696B2 |
| 출처 데이터셋 | uspto-grants-2008_10 |
| ORD ID | ord-ada438d7963c4adbb6c39fe67aac7a39 |
| 출처 메모 | uspto-grants-2008_10 |