HCID 355603, 화합물 → HCID 59816219, 화합물
반응식
[C:1]1([C:7]2[CH:13]=[CH:12][CH:11]=[C:10]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:8]=2[NH2:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:20]1[C:33]2[C:24](=[N:25][C:26]3[C:27](=O)[CH2:28][CH2:29][CH2:30][C:31]=3[CH:32]=2)[C:23](=O)[CH2:22][CH2:21]1>>[C:14]1([C:10]2[CH:11]=[CH:12][CH:13]=[C:7]([C:1]3[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=3)[C:8]=2[N:9]=[C:23]2[C:24]3[C:33](=[CH:32][C:31]4[CH2:30][CH2:29][CH2:28][C:27](=[N:9][C:8]5[C:10]([C:14]6[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=6)=[CH:11][CH:12]=[CH:13][C:7]=5[C:1]5[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=5)[C:26]=4[N:25]=3)[CH2:20][CH2:21][CH2:22]2)[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1참가 물질
3
실험 절차
was synthesized by methods similar to those in Examples 3 and 4: 2,6-diphenylaniline was condensed with 2,3,7,8-tetrahydro-1H,6H-acridine-4,5-dione to yield 4,5-bis[2,6-diphenylphenylimino]-1,2,3,4,5,6,7,8-octahydroacridine (6). Complexation of (6) with FeCl2.4H2O was carried out with azeotropic removal of methanol in benzene. The structure of final complex was proved by direct probe GC. Exact mass direct probe calculated for C49H39Cl2FeN3: 795.19. Found: 795.19.
후처리
- customwas synthesized by methods similar to those in Examples 3 and 4
출처 및 근거
- ORD 기록
- ord-65ab13d6c7a24260ad5ac6f23bb104d0