참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Chloral Hydrate | HCID 2707 | — |
| 반응물 | Chloroform | HCID 6212 | — |
| 반응물 | Homoveratrylamine | HCID 8421 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N-[2-(3,4-dimethoxyphenyl)ethyl]formamide | HCID 84337 | — |
반응 단계
First, 2-(3,4-dimethoxyphenyl)-ethylamine (181.2 g, 1 mol) and chloral hydrate (181 g, 1.1 mol) are mixed together and heated to 120° C., with stirring, for 20 minutes and any volatile components (chloroform and water) are eliminated in a water jet vacuum at an oil bath temperature of 140° C. An oil is left behind which is further processed without any purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04678792 |
|---|
| 출처 데이터셋 | uspto-grants-1987_07 |
|---|
| ORD ID | ord-e687a79b375e40ad8ca7776ad80c5a88 |
|---|
| 출처 메모 | uspto-grants-1987_07 |
|---|
