Isopropanol → HCID 20194014, 화합물

HRID 2118505노트

반응식

HRID 2118505 반응식
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]=1.[Cl:11][C:12]1[CH:19]=[CH:18][CH:17]=[CH:16][C:13]=1[CH2:14]Cl.[S:20]([O-:24])([OH:23])(=[O:22])=[O:21].C(O)(C)C>C(#N)C>[S:20]([O-:24])([OH:23])(=[O:22])=[O:21].[Cl:11][C:12]1[CH:19]=[CH:18][CH:17]=[CH:16][C:13]=1[CH2:14][N+:2]1[CH2:3][CH2:4][C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[CH:1]=1

참가 물질

6

반응물 4

HCID 3776IsopropanolHCID 119062-Chlorobenzyl chlorideHCID 61778Sulfate, hydrogenHCID 767053,4-Dihydroisoquinoline

생성물 1

HCID 20194014HCID 20194014, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

The title compound is prepared analogously to Example A from 3,4-dihydroisoquinoline and 2-chlorobenzyl chloride in acetonitrile. The melting point of the hydrogensulphate is 190°-192° C. (from isopropanol).

후처리

  1. customis 190°-192° C.

출처 및 근거

ORD 기록
ord-7a80b222e76b4858a969b9061ca94806
출처 데이터셋
uspto-grants-1987_07
특허 번호
US04678792

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