Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → 1,4-Dibromoisoquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | 1-Bromoisoquinoline | HCID 640963 | — |
| 생성물 | 1,4-Dibromoisoquinoline | HCID 640981 | — |
반응 단계
The starting material was prepared by reaction of 1-bromoisoquinoline with HBr to give 1,4-dibromoisoquinoline, m.p. 95°-96°, followed by reaction of this compound with trimethyloxonium tetrafluoroborate in CH2Cl2 to give 1,4-dibromo-2-methylisoquinolinium tetrafluoroborate; n.m.r. in solvent A: 3.5(s, 3H); 7.2-8.4(m, 5H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04678781 |
| 출처 데이터셋 | uspto-grants-1987_07 |
| ORD ID | ord-0a4a1fb55fb3423fbcaabb8d6c3586fe |
| 출처 메모 | uspto-grants-1987_07 |