참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methane | HCID 297 | — |
| 반응물 | Allyl acetate | HCID 11584 | — |
| 반응물 | Pentamethyldisiloxane | HCID 74037 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 1-Disiloxanol, 1,1,3,3,3-pentamethyl-, 1-acetate | HCID 116807 | — |
반응 단계
A mixture containing 14.8 g of 1,1,1,3,3-pentamethyldisiloxane, 10.0 g of allyl acetate (acetic acid allylester) and 0.01 g of palladium supported on activated charcoal, in which the 0.1 g refers to the total weight of the charcoal and the palladium, is heated to boiling under reflux (approximately 105° C.) for 4 hours. The 1,1,1,3,3-pentamethyl-3-acetoxydisiloxane yield is quantitative.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04680365 |
|---|
| 출처 데이터셋 | uspto-grants-1987_07 |
|---|
| ORD ID | ord-a176e21bb5f04f3c962418b03a0824fd |
|---|
| 출처 메모 | uspto-grants-1987_07 |
|---|
