Sulfuric Acid → Sulfuric acid--aniline (1/1)

HRID 2118936노트

반응식

[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:8](=[O:12])(=[O:11])([OH:10])[OH:9]>>[S:8]([OH:12])([OH:11])(=[O:10])=[O:9].[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 1118Sulfuric Acid

HCID 6115Aniline

생성물 1

HCID 3015090Sulfuric acid--aniline (1/1)

실험 절차

Aniline and sulfuric acid, in substantailly equimolar amounts are charged to the rotating reactor to form aniline hydrogen sulfate therein. When the charging is completed, the temperature within the furnace is raised to heat the reactor and its contents above the rearrangement temperature. The released water is vented through one of the hollow shafts exiting the end of reactor. The water is externally condensed.

출처 및 근거

ORD 기록: ord-8bf7be48ea91428ab4f7cc31384f34eb
출처 데이터셋: uspto-grants-1987_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04681710

반응 노트

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