4-Hydroxybenzophenone → 4-Benzoylphenyl cyclohexanecarboxylate

HRID 2119187

반응식

HRID 2119187 반응식
[OH:1][C:2]1[CH:15]=[CH:14][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[CH:16]1([C:22](Cl)=[O:23])[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1>N1C=CC=CC=1>[CH:16]1([C:22]([O:1][C:2]2[CH:3]=[CH:4][C:5]([C:6]([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)=[O:7])=[CH:14][CH:15]=2)=[O:23])[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1

참가 물질

4

반응물 2

HCID 143474-HydroxybenzophenoneHCID 75938Cyclohexanecarbonyl chloride

생성물 1

HCID 8492994-Benzoylphenyl cyclohexanecarboxylate

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

The title compound was prepared from 6.0 g of 4-hydroxybenzophenone, 6.0 ml of cyclohexanecarbonyl chloride, pyridine (70 ml). Recrystallized from ethyl acetate-ethanol-water; M.P.~111°-112° C.

후처리

  1. customRecrystallized from ethyl acetate-ethanol-water

출처 및 근거

ORD 기록
ord-55956aaa2d824ce298c4840b7b52358a
출처 데이터셋
uspto-grants-1987_07
특허 번호
US04683241

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