Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → 3-Butyl-6-formamido-phthalide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | 6-Amino-3-butyl-phthalide | HCID 9877706 | — |
| 생성물 | 3-Butyl-6-formamido-phthalide | HCID 9834570 | — |
반응 단계
A solution of 3.07 g (0.015 mol) of the compound obtained in Example 4 in 15 ml of 85% formic acid is heated to 60° C. An hour later the reaction mixture is poured into ice-water. The separated solid is collected and crystallised from dilute ethanol to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06689808B2 |
| 출처 데이터셋 | uspto-grants-2004_02 |
| ORD ID | ord-3ff838d2a1064b6aa58b0000a78b057b |
| 출처 메모 | uspto-grants-2004_02 |