HCID 23436574, 화합물 → 2-(2-Methylphenyl)-4-nitrobenzoic acid

HRID 2121153노트

반응식

HRID 2121153 반응식
C[O:2][C:3](=[O:20])[C:4]1[CH:9]=[CH:8][C:7]([N+:10]([O-:12])=[O:11])=[CH:6][C:5]=1[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[CH3:19].[OH-].[Na+].CO>>[N+:10]([C:7]1[CH:8]=[CH:9][C:4]([C:3]([OH:20])=[O:2])=[C:5]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=2[CH3:19])[CH:6]=1)([O-:12])=[O:11]

참가 물질

3

반응물 2

HCID 23436574HCID 23436574, 화합물HCID 23721981Sodium hydroxide methanol

생성물 1

HCID 234360742-(2-Methylphenyl)-4-nitrobenzoic acid

실험 절차

4-Nitro-2-(2-methylphenyl)benzoic acid methyl ester, prepared as in Example 178A, was saponified using aqueous NaOH—CH3OH to give 4-nitro-2-(2-methylphenyl)benzoic acid; HRMS calcd for C14H11NO4 257.0688, obsd 257.0699.

출처 및 근거

ORD 기록
ord-1392541159ff4065bbdbf17b1891db8a
출처 데이터셋
uspto-grants-2004_02
특허 번호
US06693123B2

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