Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dabsyl chloride → 1-(2-{1-[4-(4-Dimethylaminophenylazo)benzenesulfonyl]piperidin-4-yl}ethyl)-2-(ethoxymethyl)-6,7-dimethyl-1h-imidazo[4,5-c]pyridin-4-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dabsyl chloride | HCID 91660 | — |
| 반응물 | 2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine | HCID 12972962 | — |
| 생성물 | 1-(2-{1-[4-(4-Dimethylaminophenylazo)benzenesulfonyl]piperidin-4-yl}ethyl)-2-(ethoxymethyl)-6,7-dimethyl-1h-imidazo[4,5-c]pyridin-4-amine | HCID 10312362 | — |
반응 단계
Using the method of Examples 49-56, 4-dimethylaminoazobenzene4′-sulfonyl chloride was reacted with 2-(ethoxymethyl)-6,7-dimethyl-1-(2-piperidin-4-ylethyl)-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired product. The observed accurate mass was 619.3185.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06696465B2 |
| 출처 데이터셋 | uspto-grants-2004_02 |
| ORD ID | ord-b1fe4fd7905845ee80c7171bab0187f4 |
| 출처 메모 | uspto-grants-2004_02 |