Thionyl Chloride → HCID 54340583, 화합물

HRID 21424노트

반응식

HRID 21424 반응식
[CH2:1]([O:7][C:8]1[CH:9]=[C:10]([C:20]([OH:22])=O)[C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:12][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].S(Cl)([Cl:25])=O>>[CH2:1]([O:7][C:8]1[CH:9]=[C:10]([C:20]([Cl:25])=[O:22])[C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:12][CH:13]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

참가 물질

3

반응물 2

HCID 24386Thionyl ChlorideHCID 232890074-n-Hexyloxybiphenyl carboxylic acid

생성물 1

HCID 54340583HCID 54340583, 화합물

실험 절차

4-n-Hexyloxybiphenyl carboxylic acid (3.0 g) and an excessive amount of thionyl chloride were heated under refluxing for 6 hours. Unaltered thionyl chloride was distilled off to obtain 4-n-hexyloxybiphenyl carboxylic acid chloride.

후처리

  1. temperatureunder refluxing for 6 hours
  2. distillationUnaltered thionyl chloride was distilled off

출처 및 근거

ORD 기록
ord-7783c1004e9342cf9d5f678f9975d065
출처 데이터셋
uspto-grants-1995_06
특허 번호
US05424005

반응 노트

불러오는 중…