Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dichloromethane → 4-Octyl-biphenyl-4'-terephthalic acid chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Terephthaloyl chloride | HCID 7488 | — |
| 반응물 | 2-Dimethylaminopyridine | HCID 21885 | — |
| 반응물 | 4'-Octyl-[1,1'-biphenyl]-4-ol | HCID 14047211 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 4-Octyl-biphenyl-4'-terephthalic acid chloride | HCID 131719017 | — |
반응 단계
To a solution of 4-hydroxy-4'-octylbiphenyl (0.5 g) and terephthaloyl chloride (0.36 g) in about dichloromethane (30 ml) was added drop by drop triethylamine (0.2 g). To the solution was added dimethylaminopyridine (0.013 g) and the mixture was stirred at the room temperature for 10 hours to obtain the titled compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05424005 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-2394b2dec9d049a3b2e5b53f9d321778 |
| 출처 메모 | uspto-grants-1995_06 |