Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 3-Methylbenzoyl chloride | HCID 74375 | — |
| 반응물 | N-(tert-butyl)benzohydrazide | HCID 1275961 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine | HCID 15294604 | — |
반응 단계
To a stirred mixture of N'-t-butyl-N'-benzoylhydrazine (1.0 g) in 15 ml toluene and aqueous sodium hydroxide (0.5 g of 50% NaOH) was added 3-toluoyl-chloride (0.9 g). After stirring for 2 hours, the product was isolated by filtration to give N'-t-butyl-N-(3-toluoyl)-N'-benzoylhydrazine in good yield: m.p. 111°-114° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05424333 |
| 출처 데이터셋 | uspto-grants-1995_06 |
| ORD ID | ord-32bba065ba434b10a71460d0eeef938b |
| 출처 메모 | uspto-grants-1995_06 |