참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,3-Dichloro-5,6-dicyano-1,4-benzoquinone | HCID 6775 | — |
| 반응물 | 4-Hydroxycyclopent-2-en-1-yl acetate | HCID 4428208 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 4-Oxocyclopent-2-en-1-yl acetate | HCID 343117 | — |
반응 단계
144 milligrams of optically inactive 3-acetoxy-5-hydroxycyclopent-1-ene prepared as in Example 1 and 460 milligrams of 2,3-dichloro-5,6-dicyano-p-benzoquinone (DDQ) were dissolved in 5 milliliters of dioxane, after which the resulting solution was heated with stirring for 48 hours at 60° C. The precipitate separating out after the reaction was separated by filtration, and the filtrate was concentrated under reduced pressure to obtain a crude product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04132726 |
|---|
| 출처 데이터셋 | uspto-grants-1979_01 |
|---|
| ORD ID | ord-3cecaeee6024494b85d3d4b2fca34825 |
|---|
| 출처 메모 | uspto-grants-1979_01 |
|---|
