HCID 788030, 화합물 → HCID 178442913, 화합물

HRID 2163280노트

반응식

HRID 2163280 반응식
Cl.[Cl:2][C:3]1[CH:9]=[C:8]([Cl:10])[C:7]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])=[CH:6][C:4]=1[NH2:5].[Cl:30][C:31]1[CH:36]=[C:35]([Cl:37])[CH:34]=[C:33]([Cl:38])[C:32]=1[N:39]1[C:43](=[O:44])[CH2:42][C:41](OCC)=[N:40]1.ClC1C=C(Cl)C(OCCCCCCCCCCCCCCCC)=CC=1N>>[Cl:38][C:33]1[CH:34]=[C:35]([Cl:37])[CH:36]=[C:31]([Cl:30])[C:32]=1[N:39]1[C:43](=[O:44])[CH2:42][C:41]([NH:5][C:4]2[CH:6]=[C:7]([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[C:8]([Cl:10])=[CH:9][C:3]=2[Cl:2])=[N:40]1

참가 물질

4

반응물 3

HCID 788030HCID 788030, 화합물HCID 22753008HCID 22753008, 화합물HCID 22753010HCID 22753010, 화합물

생성물 1

HCID 178442913HCID 178442913, 화합물

실험 절차

Using 18 g of 2,4-dichloro-5-octadecyloxyaniline hydrochloride and 13 g of 1-(2,4,6-trichlorophenyl)-3-ethoxy-2-pyrazolin-5-one, which were prepared in a manner similar to Steps (1) and (2) of Synthesis Example 1, similar procedures to Step (3) of Synthesis Example 1, were carried out and recrystallization was performed from 100 ml of ethanol to obtain 15 g of the desired coupler. The melting point thereof was 98 to 99° C.

후처리

  1. customrecrystallization
  2. customto obtain 15 g of the desired coupler
  3. customthereof was 98 to 99° C.

출처 및 근거

ORD 기록
ord-a92ff28b31974f28909647b4998059e3
출처 데이터셋
uspto-grants-1979_01
특허 번호
US04133686

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